There's a book I have on the shelf (and have read) called, "150 and More Basic NMR Experiments: A Practical Course", and in my case it is the 2nd Completely Revised and Enlarged Edition by Siegmar Braun, Hans-Otto Kalinowski, & Stefan Berger. Are you already familiar with its material? If so, you should provide those relevant details here in your question. What you've written here is, in my opinion only, sufficiently incomplete that useful answers are improbable.
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